Development and Mechanistic Understanding of Ball Milling as a Sustainable Alternative to Traditional Synthesis

Released on by William C. Shearouse
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  • Development and Mechanistic Understanding of Ball Milling as a Sustainable Alternative to Traditional Synthesis Book Detail

  • Author : William C. Shearouse
  • Release Date : 2012
  • Publisher :
  • Genre :
  • Pages : 175
  • ISBN 13 :
  • File Size : 40,40 MB
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Development and Mechanistic Understanding of Ball Milling as a Sustainable Alternative to Traditional Synthesis by William C. Shearouse PDF Summary

Book Description: As environmental regulations become more stringent, the industrial chemical community needs methods that are sustainable, yet parallel the modern advances of organic synthesis. We believe we are solving the solution to this global problem through the development of sustainable synthesis that utilizes ball milling. Ball milling, unlike traditional synthetic methods, uses mechanical energy to drive organic reactions and transformations towards completion. Not only are we interested in finding reaction pathways that produce desired organic products in high yields, but also we are interested in understanding the mechanisms and theory of these processes in hopes that we may develop chemistries that have synthetic outcomes that are not attainable under traditional synthetic techniques. As a group, we each target different areas of "known" organic synthesis, in order to develop parallel routes that utilize sustainable, ball milling practices. Ball milling and green chemistry are introduced and described in Chapter 1. This dissertation describes specifically my efforts towards the aforementioned goals. Largely, my efforts focused on the development of sustainable olefination reactions, namely, the Wittig reaction and Horner-Wadsworth-Emmons reactions described in Chapters 3 and 4 respectively. In addition, portions of my dissertation research sought to expand the capability of ball milling reactions through the engineering and development of new ball milling tools. The use of functional resins as purification tools for ball milling reactions, described in Chapter 5, as well as the design and fabrication of vials made from different materials, described in Chapter 2, complete my dissertation research.

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